Partial recipeSource: Main
Route 1: Electrochemical
main pp.1-2, article pp.447-448 · Synthesis paragraph
Metal precursorsTris-oxalate Cr(III) complex (0.01 M) and Mn(II) ion, Cr complex:Mn ratio 2:3.
Linker precursorsOxalate supplied by the tris-oxalate Cr(III) complex; BEDT-TTF organic donor suspension.
SolventsMethanol/benzonitrile/dichloromethane solution.
AtmosphereNot reported.
Time168
Substrate orientationPlatinum electrode; orientation not reported.
Oxidant / reductantBEDT-TTF was slowly electrooxidised at a constant current of 0.1 mA.
Work-upThin shiny brown plates were collected from the platinum electrode after one week.
ActivationNone reported.
Scalability contextSingle crystals grown over one week by electrocrystallisation; no scale, yield or batch size reported.
Show 8 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | tris-oxalate Cr(III) complex | 0.01 M | main pp.1-2, article pp.447-448 · Synthesis paragraph |
| Metal Source | Mn(II) ion | ratio to tris-oxalate Cr(III) complex 3:2 as written in text as Cr complex and Mn(II) ion in a ratio 2:3 | main pp.1-2, article pp.447-448 · Synthesis paragraph |
| Linker | oxalate | contained in tris-oxalate Cr(III) complex | main pp.1-2, article pp.447-448 · Synthesis paragraph |
| Other | BEDT-TTF | suspension | main pp.1-2, article pp.447-448 · Synthesis paragraph |
| Solvent | methanol | Not specified | main pp.1-2, article pp.447-448 · Synthesis paragraph |
| Solvent | benzonitrile | Not specified | main pp.1-2, article pp.447-448 · Synthesis paragraph |
| Solvent | dichloromethane | Not specified | main pp.1-2, article pp.447-448 · Synthesis paragraph |
| Electrolyte | constant-current electrocrystallisation at 0.1 mA | Not specified | main pp.1-2, article pp.447-448 · Synthesis paragraph |