Microscopy Morphology — 3D self-branched zinc-cobalt Oxide@N-doped carbon hollow nanowall arrays for high-performance asymmetric supercapacitors and oxygen electrocatalysis

4 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Co-MOF/CTs · Electrode

Co-MOF nanowall arrays grown on CTs; thickness estimated from enlarged SEM view.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co-MOF nanowall thickness	average thickness of around 185 nm	185 nm	around	Text Approximate	655 · 3. Results and discussion · Fig. S2b-c

Co-MOF nanowall arrays on Fe foil, Ni foam and graphite paper · Thin Film

Substrate generality of Co-MOF nanowall array growth on Fe foil, Ni foam and graphite paper.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co-MOF growth on alternative substrates	Co-MOF nanowall arrays can grow on Fe foil, Ni foam and graphite paper	—	—	Text Qualitative	655 · 3. Results and discussion · Fig. S4

3D self-branched ZnCo2O4@NC/CTs · Electrode

Morphology, hollow structure, lattice spacing and elemental distribution of Co-MOF-derived ZnCo2O4@NC nanowalls.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
EDS elemental distribution	Zn, Co, N, C and O uniformly distributed on nanowall array	—	—	Text Qualitative	656 · 3. Results and discussion · Fig. 2g
Zn/Co atomic ratio	about 2.0	2 dimensionless	about	Text Approximate	656 · 3. Results and discussion · Fig. 2g(viii)
ZnCo2O4 lattice spacing (111)	0.47 nm	0.47 nm	—	Text Rounded Reported	656 · 3. Results and discussion · Fig. 2f
ZnCo2O4 lattice spacing (311)	0.24 nm	0.24 nm	—	Text Rounded Reported	656 · 3. Results and discussion · Fig. 2f
target morphology	3D self-branched hollow nanowall arrays with porous ZnCo2O4 nanoflakes on hollow NC nanowalls	—	—	Text Qualitative	656 · 3. Results and discussion · Fig. 2a-c
ZnCo2O4 nanoparticle diameter in nanoflakes	~10 nm in diameter	10 nm	~	Text Approximate	656 · 3. Results and discussion · Fig. 2f

ZnCo-MOF/CTs etching-time series (10, 20, 30 and 60 min) · Electrode

ZnCo-MOF/CTs precursor morphology and elemental content compared after 10, 20, 30 and 60 min Zn2+ exchange/etching.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
effect of ZnCo-MOF etching time on morphology	short-time etching causes insufficient/semi-hollow structures; excess Zn(NO3)2 causes nanoflake overgrowth and severe etching/destruction	—	—	Text Qualitative	656 · 3. Results and discussion · Fig. S6-S7