Spectroscopy — Engineering defective trimetallic metal-organic framework nanosheets for advanced water oxidation electrocatalysis

3 measurement groups · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

NiFeZn-1 MOF nanosheets · Nanosheet

NiFeZn-1 and NiFeZn-5 compositional comparison

Context: pristine MOF nanosheet catalyst/electrode ink unless otherwise noted
Measurement source: 3 · Results and discussion 3.1 · Fig. S4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
NiFeZn-1 Ni/Fe/Zn molar ratio	75.4:19.6:5.0	—	—	Text Exact Reported	3 · Results and discussion 3.1 · Fig. S4
NiFeZn-5 Ni/Fe/Zn molar ratio	60.2:14.4:25.5	—	—	Text Exact Reported	3 · Results and discussion 3.1 · Fig. S4

NiFeZn MOF nanosheets · Nanosheet

elemental composition of as-synthesised NiFeZn MOF nanosheets

Context: pristine MOF nanosheet catalyst/electrode ink unless otherwise noted
Measurement source: 3 · Results and discussion 3.1 · Fig. 1f-l

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
SEM-EDS Fe atomic ratio component	Ni/Fe/Zn = 63.6:19.0:17.4	—	—	Text Exact Reported	3 · Results and discussion 3.1 · Fig. 1f
SEM-EDS Ni atomic ratio component	Ni/Fe/Zn = 63.6:19.0:17.4	—	—	Text Exact Reported	3 · Results and discussion 3.1 · Fig. 1f
SEM-EDS Zn atomic ratio component	Ni/Fe/Zn = 63.6:19.0:17.4	—	—	Text Exact Reported	3 · Results and discussion 3.1 · Fig. 1f

NiFeZn MOF nanosheets · Nanosheet

surface elements and chemical valence states

Context: pristine MOF nanosheet catalyst/electrode ink unless otherwise noted
Measurement source: 3 · Results and discussion 3.1 · Fig. 2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Zn 2p binding energy	1045.2 eV	—	—	Text Exact Reported	3 · Results and discussion 3.1 · Fig. 2d
Zn 2p binding energy	1021.9 eV	—	—	Text Exact Reported	3 · Results and discussion 3.1 · Fig. 2d