Diffraction Structure — Single-Atom Catalysts in Conductive Metal-Organic Frameworks: Enabling Reversible Gas Sensing at Room Temperature

Measurement evidence

Diffraction Structure

Single-Atom Catalysts in Conductive Metal-Organic Frameworks: Enabling Reversible Gas Sensing at Room Temperature · Park C., Shin H., Jeon M. et al. · ACS Nano · 2024

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Ex-situ XRD before and after NO2 exposure

Pd1-cMOF powder · Powder

Pristine cMOF and Pd1-cMOF compared before and after NO2 exposure.

Atmosphere
NO2 exposure followed by ex-situ XRD
Context
Pd1-cMOF target compared with pristine cMOF control.
Measurement source
rendered page 23 / SI p.23 · Figure S20 · Figure S20
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Pristine cMOF (100) XRD peak relative intensity after NO2reduced to 56%Text
Exact Reported
rendered page 23 / SI p.23 · Figure S20 · Figure S20
Pd1-cMOF (100) XRD peak relative intensity after NO2Marked as a best value within this paperreduction alleviated to 73%Text
Exact Reported
rendered page 23 / SI p.23 · Figure S20 · Figure S20

Powder X-ray diffraction (XRD), Cu K-alpha, lambda = 1.5418 A

Pd1-cMOF powder · Powder

XRD of pristine cMOF, Pd1-cMOF, Ir1-cMOF, Ag1-cMOF and Pd-NP@cMOF to assess structural retention.

Context
Target and composite samples compared with pristine Cu3(HITP)2.
Measurement source
rendered page 4 / article p.26069 · Characterization of SACs Stabilized in cMOF · Figure 3a; Figures S9, S10c and S20
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Pd1-cMOF XRD structural retentionprimary Cu3(HITP)2 peaks retained with no significant intensity changeText
Qualitative
rendered page 4 / article p.26069 · Characterization of SACs Stabilized in cMOF · Figure 3a