Other — Multifunctional coordination polymers based on copper(i) and mercaptonicotinic ligands: Synthesis, and structural, optical and electrical characterization

Measurement evidence

Other

Multifunctional coordination polymers based on copper(i) and mercaptonicotinic ligands: Synthesis, and structural, optical and electrical characterization · Hassanein K., Cappuccino C., Amo-Ochoa P. et al. · Dalton Transactions · 2020 · 10545-10553

3 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

thermogravimetric analysis

CP1 orange solid from method A · Powder

PerkinElmer TGA7; 35-400 C under N2 gas flow; heating rate 5 C min^-1

Temperature
308-673
Atmosphere
N2
Geometry
bulk solid/powder
Context
pristine CP1
Measurement source
7 · Experimental - Materials and methods · Figure S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
thermal decomposition onset statementthermal decomposition takes place at temperatures over 423 K423 KText
Approximate
5 · Electrical characterization · Figure S4

thermogravimetric analysis

CP2 orange/red crystals · Single Crystal

PerkinElmer TGA7; 35-400 C under N2 gas flow; heating rate 5 C min^-1

Temperature
308-673
Atmosphere
N2
Geometry
bulk crystals/powder
Context
pristine CP2
Measurement source
3, 7 · Results and discussion; Experimental - Materials and methods · Figure S5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
first TGA mass loss intervalDelta Y = 21.3166% from about 174.40 to 255.30 CVisual Estimate
Approximate
4 · TGA · Figure S5

thermogravimetric analysis

CP3 yellow crystals from method A · Single Crystal

PerkinElmer TGA7; 35-400 C under N2 gas flow; heating rate 5 C min^-1

Temperature
308-673
Atmosphere
N2
Geometry
bulk crystals/powder
Context
pristine CP3
Measurement source
3, 7 · Results and discussion; Experimental - Materials and methods · Figure S6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
first TGA mass loss intervalDelta Y = 5.5919% from about 168.47 to 225.37 CVisual Estimate
Approximate
4 · TGA · Figure S6