Microscopy Morphology — Immobilization of N-(3-aminopropyl)-imidazole through MOFs in proton conductive membrane for elevated temperature anhydrous applications

Measurement evidence

Microscopy Morphology

Immobilization of N-(3-aminopropyl)-imidazole through MOFs in proton conductive membrane for elevated temperature anhydrous applications · Wu B., Liang G., Lin X. et al. · Journal of Membrane Science · 2014 · 86-95

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM, XT30 ESEM-TMP PHILIP

6% encapsulated MOFs membrane · Thin Film

SEM images of MOFs, MOFs>NAPI and membrane cross-sections

Geometry
dried, gold-coated membrane cross-sections
Context
composite membrane compared with pristine and guest-loaded MOFs
Measurement source
p006 · 3.5 SEM and TEM morphology · Fig. 7
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
MOF crystal morphologyoctagonal structureText
Qualitative
p006 · 3.5 SEM and TEM morphology · Fig. 7
NAPI adsorption locationinterior and outer surface of frameworksText
Qualitative
p006 · 3.5 SEM and TEM morphology · Fig. 7

TEM, Hitachi H7600, 80 kV

6% encapsulated MOFs membrane · Thin Film

Stained SPPO-MOFs>NAPI, pristine SPPO, SPPO-MOFs without NAPI and SPPO-NAPI membranes; sections 60-100 nm

Geometry
ultramicrotomed slices on copper grids
Context
target membrane and polymer/composite controls
Measurement source
p001-p002 · SI 2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
ionic-domain size3-5 nmText
Range
p007 · 3.5 SEM and TEM morphology · Fig. 8
TEM section thickness60-100 nmText
Range
p001 · SI 2
TEM accelerating voltage80 kVText
Exact Reported
p001 · SI 2