Spectroscopy — Fabrication of 3D Co-doped Ni-based MOF hierarchical micro-flowers as a high-performance electrode material for supercapacitors

Measurement evidence

Spectroscopy

Fabrication of 3D Co-doped Ni-based MOF hierarchical micro-flowers as a high-performance electrode material for supercapacitors · Wang J., Zhong Q., Xiong Y. et al. · Applied Surface Science · 2019 · 1158-1165

3 measurement groups · 12 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

energy dispersive X-ray spectroscopy

Co2-Ni-MOF powder · Powder

EDS analysis of Co2-Ni-MOF material shown in SI Fig. S4.

Context
Co-doped MOF powder.
Measurement source
4 · 3.1 Structure and morphology characterization · Fig. S4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
EDS confirmation of Ni and Co elementsexistence of both Ni and Co elementsText
Qualitative
4 · 3.1 Structure and morphology characterization · Fig. S4

Fourier transform infrared spectroscopy

Ni-MOF powder · Powder

FTIR spectra measured for Ni-MOF and Cox-Ni-MOF materials.

Context
Pristine and Co-doped MOF powders.
Measurement source
2 · 2.2 Characterization · Fig. S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
carboxylate antisymmetric vibration1580 cm-1Text
Rounded Reported
4 · 3.1 Structure and morphology characterization · Fig. S1
carboxylate symmetric vibration1380 cm-1Text
Rounded Reported
4 · 3.1 Structure and morphology characterization · Fig. S1
O-H stretching vibration FTIR peak3590 cm-1Text
Rounded Reported
4 · 3.1 Structure and morphology characterization · Fig. S1

X-ray photoelectron spectroscopy

Co2-Ni-MOF powder · Powder

XPS survey and high-resolution Ni 2p / Co 2p spectra comparing Ni-MOF and Co2-Ni-MOF.

Context
Powder MOFs.
Measurement source
4 · 3.1 Structure and morphology characterization · Fig. 3
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Co2-Ni-MOF surface carbon atomic percentage47.39%Text
Exact Reported
5 · 3.1 Structure and morphology characterization · Fig. 3
Co2-Ni-MOF surface cobalt atomic percentage0.53%Text
Exact Reported
5 · 3.1 Structure and morphology characterization · Fig. 3
Co2-Ni-MOF surface nickel atomic percentage13.38%Text
Exact Reported
5 · 3.1 Structure and morphology characterization · Fig. 3
Co2-Ni-MOF surface oxygen atomic percentage37.04%Text
Exact Reported
5 · 3.1 Structure and morphology characterization · Fig. 3
Co 2p1/2 binding energy796.93 eVText
Exact Reported
5 · 3.1 Structure and morphology characterization · Fig. 3c
Co 2p3/2 binding energy781.73 eVText
Exact Reported
5 · 3.1 Structure and morphology characterization · Fig. 3c
Ni 2p1/2 binding energy873.9 eVText
Rounded Reported
4 · 3.1 Structure and morphology characterization · Fig. 3b
Ni 2p3/2 binding energy856.3 eVText
Rounded Reported
4 · 3.1 Structure and morphology characterization · Fig. 3b