Spectroscopy — One-Step Solvothermal Synthesis of Raspberry-like NiCo-MOF for High-Performance Flexible Supercapacitors for a Wide Operation Temperature Range

Measurement evidence

Spectroscopy

One-Step Solvothermal Synthesis of Raspberry-like NiCo-MOF for High-Performance Flexible Supercapacitors for a Wide Operation Temperature Range · Zhang W., Shahnavaz Z., Yan X. et al. · Inorganic Chemistry · 2022 · 15287-15301

2 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR and Raman spectroscopy

Infrared spectroscopy Raman spectroscopy

NiCo-MOF-3 powder · Powder

Functional groups and vibrational modes of NiCo-MOF samples.

Geometry: powder
Context: pristine mixed-metal MOF powder
Measurement source: 15291 / p005 · 3.1 Morphologies and Compositions · Figure 2d,e

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
FTIR carbonyl stretching peak	1610 cm^-1	—	—	Text Rounded Reported	15291 / p005 · 3.1 Morphologies and Compositions · Figure 2e
FTIR/Raman Ni-O and Co-O vibrations	413 and 630 cm^-1	—	—	Text Rounded Reported	15291 / p005 · 3.1 Morphologies and Compositions · Figure 2d
FTIR O-H vibration peak	3420 cm^-1	—	—	Text Rounded Reported	15291 / p005 · 3.1 Morphologies and Compositions · Figure 2e

X-ray photoelectron spectroscopy (XPS), Al Kalpha radiation

X-ray photoelectron spectroscopy

NiCo-MOF-3 powder · Powder

Elemental composition and valence states of NiCo-MOF-3.

Geometry: powder
Context: pristine mixed-metal MOF powder
Measurement source: 15291 / p005 · 3.1 Morphologies and Compositions · Figure 3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co 2p1/2 binding energy	797.2 eV	—	—	Text Rounded Reported	15291 / p005 · 3.1 Morphologies and Compositions · Figure 3c
Co 2p3/2 binding energy	781.9 eV	—	—	Text Rounded Reported	15291 / p005 · 3.1 Morphologies and Compositions · Figure 3c
XPS detected elements	Ni, Co, O, C, and N	—	—	Text Qualitative	15291 / p005 · 3.1 Morphologies and Compositions · Figure 3a
N 1s -NH- peak	400.0 eV	—	—	Figure Axis Approximate	15289 / p003 · Figure 3 · Figure 3e
Ni 2p1/2 binding energy	874.0 eV	—	—	Text Rounded Reported	15291 / p005 · 3.1 Morphologies and Compositions · Figure 3b
Ni 2p3/2 binding energy	856.3 eV	—	—	Text Rounded Reported	15291 / p005 · 3.1 Morphologies and Compositions · Figure 3b
O 1s metal-oxygen peak	531.6 eV	—	—	Text Rounded Reported	15292 / p006 · 3.1 Morphologies and Compositions · Figure 3f