SEM, TEM, EELS elemental mapping, and powder XRD
X-ray diffraction and scatteringScanning electron microscopyTransmission electron microscopyElemental microanalysis and mapping
hollow Zn0.30Co2.70S4 · Powder
Hollow sulphide morphology, spinel phase, shell thickness, particle shell nanostructure and EELS distribution.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| sulphide shell nanoparticle size | ca. 20 nm | — | ca. | Text Approximate | 1361 · 3.2 · Figure 2d; Figure S5b |
| sulphide phase assignment | indexed as cubic Co3S4, Powder Diffraction File No. 47-1738 | — | — | Text Qualitative | 1361 · 3.2 · Figure 3a |
| Zn0.30Co2.70S4 shell thickness | ca. 30-50 nm | — | range 30-50 nm | Text Range | 1361 · 3.2 · Figure 2c,d |