N2 adsorption isotherm, BET analysis; Zeo++ geometric analysis
Activated Ni-3D-ox · Powder
Sample activated at 100 C under high dynamic vacuum (<10^-4 mbar) for 24 h before N2 isotherm at 77 K; additional main-text discussion of activation at 110 C.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Ni-1D BET surface area | 33.57 +/- 0.28 m2/g | — | +/- 0.28 | Caption Exact Reported | SI p.38 · Figure S24 · Figure S24 |
| Ni-3D-ox BET apparent surface area | 119.61 +/- 0.46 m2/g | — | +/- 0.46 | Caption Exact Reported | SI p.38 · Figure S24 · Figure S24 |
| Ni-3D-ox theoretical solvent-accessible surface area | 518 m2/g | — | — | Text Exact Reported | SI p.39 · Figure S25 discussion · Figure S25 |