Complete recipeSource: Main
Route 1: Hydrothermal
2 · 2.3. Preparation of the adsorbent
Metal precursors1.19 g zinc nitrate hexahydrate
Linker precursors0.473 g benzimidazole
Solvents90 mL DMF; methanol workup
Atmospheresealed Teflon autoclave; atmosphere not otherwise specified
Temperature130
Time24
Work-upSolid soaked in methanol for 24 h at room temperature to remove DMF/unreacted chemicals; methanol decanted; crystals dried at room temperature for 24 h.
ActivationDried for another 24 h under vacuum at 160 C.
Scalability context150 mL Teflon autoclave batch synthesis.
Show 4 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | zinc nitrate hexahydrate | 1.19 g | 2 · 2.3. Preparation of the adsorbent |
| Linker | benzimidazole | 0.473 g | 2 · 2.3. Preparation of the adsorbent |
| Solvent | DMF | 90 mL | 2 · 2.3. Preparation of the adsorbent |
| Solvent | methanol | soaked for 24 h | 2 · 2.3. Preparation of the adsorbent |