Diffraction Structure — Regulating Electronic Structure of Bimetallic NiFe-THQ Conductive Metal–Organic Frameworks to Boost Catalytic Activity for Oxygen Evolution Reaction

Measurement evidence

Diffraction Structure

Regulating Electronic Structure of Bimetallic NiFe-THQ Conductive Metal–Organic Frameworks to Boost Catalytic Activity for Oxygen Evolution Reaction · Zhao L., Yan J., Huang H. et al. · Advanced Functional Materials · 2024 · 2310902

2 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Rietveld refinement of XRD

X-ray diffraction and scattering

Fe-THQ · Powder

Fe-THQ used as structural analysis example; cubic Pm-3 model.

Context: pristine Fe-THQ powder
Measurement source: p017 · S2 Supplementary Figures and Tables · Table S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Fe-THQ a lattice parameter	10.615	—	—	SI Table Exact Reported	p017 · S2 Supplementary Figures and Tables · Table S2
Fe-THQ alpha/beta/gamma	90	—	—	SI Table Exact Reported	p017 · S2 Supplementary Figures and Tables · Table S2
Fe-THQ b lattice parameter	10.615	—	—	SI Table Exact Reported	p017 · S2 Supplementary Figures and Tables · Table S2
Fe-THQ c lattice parameter	10.615	—	—	SI Table Exact Reported	p017 · S2 Supplementary Figures and Tables · Table S2
Fe-THQ goodness of fit chi2	4.56	—	—	SI Table Exact Reported	p017 · S2 Supplementary Figures and Tables · Table S2
Fe-THQ Rp	2.03	—	—	SI Table Exact Reported	p017 · S2 Supplementary Figures and Tables · Table S2
Fe-THQ Rwp	2.56	—	—	SI Table Exact Reported	p017 · S2 Supplementary Figures and Tables · Table S2
Fe-THQ unit cell volume	1196.14	—	—	SI Table Exact Reported	p017 · S2 Supplementary Figures and Tables · Table S2

powder X-ray diffraction

X-ray diffraction and scattering

NixFe1-x-THQ series · Powder

Cu Kalpha radiation; series XRD patterns compared with simulated/refined patterns.

Context: pristine c-MOF powder series
Measurement source: p002 · 2.1 Material Synthesis and Structural Characterizations · Figure 1d

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
(100) diffraction peak	8.26 degrees 2theta	—	—	Text Rounded Reported	p002 · 2.1 Material Synthesis and Structural Characterizations · Figure 1d
(200) diffraction peak	16.55 degrees 2theta	—	—	Text Rounded Reported	p002 · 2.1 Material Synthesis and Structural Characterizations · Figure 1d
(300) diffraction peak	25.94 degrees 2theta	—	—	Text Rounded Reported	p002 · 2.1 Material Synthesis and Structural Characterizations · Figure 1d