Diffraction Structure — Two-dimensional conductive metal-organic frameworks with dual metal sites toward the electrochemical oxygen evolution reaction

4 measurement groups · 11 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

NiPc-Ni powder/nanosheets · Nanosheet

PANalytical Empyrean, Cu Kalpha radiation 1.540598 Angstrom, 40 kV, 40 mA; structure compared with DFT-optimised eclipsed AA stacking.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
lattice parameter a	17.8963 Angstrom	—	—	SI Table Exact Reported	5 · PXRD Measurements · Table S1
lattice parameter c	3.4372 Angstrom	—	—	SI Table Exact Reported	5 · PXRD Measurements · Table S1
assigned PXRD peaks	4.9, 7.0, 9.9 and 26.5 degrees 2theta assigned to (100), (110), (200) and (001)	—	—	Text Rounded Reported	1624 · Synthesis and characterization · Fig. 2
Pawley refinement Rwp	Rwp of 2.78%	—	—	Text Exact Reported	1624 · Synthesis and characterization · Fig. 2
space group	P4/mmm	—	—	Text Exact Reported	1624 · Synthesis and characterization · Fig. 2

NiPc-Zn powder · Powder

PXRD pattern and simulated lattice parameters reported in SI Table S1/Fig. S4.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
lattice parameter a	17.9504 Angstrom	—	—	SI Table Exact Reported	5 · PXRD Measurements · Table S1
lattice parameter c	3.4317 Angstrom	—	—	SI Table Exact Reported	5 · PXRD Measurements · Table S1

ZnPc-Ni powder · Powder

PXRD pattern and simulated lattice parameters reported in SI Table S1/Fig. S4.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
lattice parameter a	17.9396 Angstrom	—	—	SI Table Exact Reported	5 · PXRD Measurements · Table S1
lattice parameter c	3.4337 Angstrom	—	—	SI Table Exact Reported	5 · PXRD Measurements · Table S1

ZnPc-Zn powder · Powder

PXRD pattern and simulated lattice parameters reported in SI Table S1/Fig. S4.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
lattice parameter a	17.9936 Angstrom	—	—	SI Table Exact Reported	5 · PXRD Measurements · Table S1
lattice parameter c	3.4283 Angstrom	—	—	SI Table Exact Reported	5 · PXRD Measurements · Table S1