Microscopy Morphology — Enhancing the Electrochemical Energy Storage of Metal-Organic Frameworks: Linker Engineering and Size Optimization

Measurement evidence

Microscopy Morphology

Enhancing the Electrochemical Energy Storage of Metal-Organic Frameworks: Linker Engineering and Size Optimization · Hang X., Wang X., Chen J. et al. · Inorganic Chemistry · 2025 · 427-434

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM, TEM, HAADF-STEM elemental mapping

Scanning electron microscopy Transmission electron microscopy Elemental microanalysis and mapping

Primary Ni-MOF powder series · Powder

FESEM Zeiss-Supra55; TEM JEM-2100; HRTEM/element mapping on Tecnai G2 F30 S-TWIN

Geometry: powder/nanorod imaging
Context: pristine Ni-MOF powders
Measurement source: S2 · Materials and Characterization

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Elemental mapping uniformity	Ni, S, O, N, and C showed a uniform distribution in Ni-tdc-bpe and Ni-tdc-bpe(0.5)	—	—	Text Qualitative	428 · Results and Discussion · Figure 1i,j
Ni-tdc-bpe(0.5) nanorod diameterMarked as a best value within this paper	about 35 nm	—	about	Text Approximate	428 · Results and Discussion · Figure 1d
Ni-tdc-bpe nanorod diameter	about 55 nm	—	about	Text Approximate	428 · Results and Discussion · Figure 1b
Ni-tdc-bpe nanorod length	about 280 nm	—	about	Text Approximate	428 · Results and Discussion · Figure 1b
Ni-tdc-bpy(0.5) nanorod diameter	about 70 nm	—	about	Text Approximate	428 · Results and Discussion · Figure 1c
Ni-tdc-bpy nanorod diameter	about 100 nm	—	about	Text Approximate	428 · Results and Discussion · Figure 1a
Ni-tdc-bpy nanorod length	about 240 nm	—	about	Text Approximate	428 · Results and Discussion · Figure 1a

SEM and GCD for 0.25/0.75 variants

Scanning electron microscopy Galvanostatic cycling

Ni-tdc-bpy/bpe 0.25 and 0.75 size variants · Powder

SEM images for 0.75 and 0.25 variants; GCD curves for 0.25 variants at 0.5-5 A/g

Geometry: powder SEM and composite electrodes
Context: SI-only pristine variants and electrodes
Measurement source: S5, S18 · Figure captions · Figures S1 and S14

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
SI-only 0.25/0.75 variant measurements	SEM shown for Ni-tdc-bpy(0.75), Ni-tdc-bpe(0.75), Ni-tdc-bpy(0.25), and Ni-tdc-bpe(0.75); GCD shown for Ni-tdc-bpy(0.25) and Ni-tdc-bpe(0.25)	—	—	Caption Qualitative	S5, S18 · Figure captions · Figures S1 and S14