Partial recipeSource: Main
Route 1: Hydrothermal
2 · 2.1 Synthesis
Metal precursorsCuCl2.2H2O (0.51 g)
Linker precursors1,2,4-triazole (0.27 g)
SolventsWater (20 mL)
AdditivesNaF (0.20 g), H3PO4 85 wt% (0.72 g), KOH solution 6.3 M (2.75 mL)
AtmosphereAutogenous pressure in sealed Teflon-lined stainless steel autoclave; gas atmosphere not otherwise reported.
Temperature180
Time120-144
Work-upAfter cooling, product recovered by filtration, washed thoroughly with water and dried at 60 C overnight.
ActivationNo separate activation reported.
Show 6 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | CuCl2.2H2O | 0.51 g | 2 · 2.1 Synthesis |
| Solvent | water | 20 mL | 2 · 2.1 Synthesis |
| Additive | NaF | 0.20 g | 2 · 2.1 Synthesis |
| Linker | 1,2,4-triazole | 0.27 g | 2 · 2.1 Synthesis |
| Acid | H3PO4 | 0.72 g · 85 wt% | 2 · 2.1 Synthesis |
| Base | KOH solution | 2.75 mL · 6.3 M | 2 · 2.1 Synthesis |