Diffraction Structure — Creating Dual Active Sites in Conductive Metal-Organic Frameworks for Efficient Water Splitting

Measurement evidence

Diffraction Structure

Creating Dual Active Sites in Conductive Metal-Organic Frameworks for Efficient Water Splitting · He Y., Yan F., Zhang X. et al. · Advanced Energy Materials · 2023 · 2204177

2 measurement groups · 8 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

XRD, SEM, HRTEM, elemental mapping, ICP, XPS

X-ray photoelectron spectroscopy X-ray diffraction and scattering Scanning electron microscopy Transmission electron microscopy Elemental microanalysis and mapping Bulk elemental and compositional analysis

IrCo-CAT/CC nanorod arrays · Electrode

Characterisation of IrCo-CAT/CC and RhCo-CAT/CC analogues.

Geometry: nanorod arrays on carbon cloth
Context: target_samples
Measurement source: article p.5 · Results and Discussion · Figures S12-S17 referenced

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
IrCo-CAT and RhCo-CAT nanorod diameter	about 80.0 nm	—	—	Text Approximate	article p.5 · Results and Discussion · Figure S13 referenced
IrCo-CAT and RhCo-CAT nanorod length	about 1.2 micrometre	—	—	Text Approximate	article p.5 · Results and Discussion · Figure S13 referenced
Co content in IrCo-CAT	19.8 wt%	—	—	SI Table Exact Reported	S28-S29 · Table S3 · Table S3
Ir content in IrCo-CAT	0.5 wt%	—	—	SI Table Exact Reported	S28-S29 · Table S3 · Table S3
Co content in RhCo-CAT	19.4 wt%	—	—	SI Table Exact Reported	S28-S29 · Table S3 · Table S3
Rh content in RhCo-CAT	0.8 wt%	—	—	SI Table Exact Reported	S28-S29 · Table S3 · Table S3

X-ray diffraction (XRD)

X-ray diffraction and scattering

RuCo-CAT/CC nanorod arrays · Electrode

XRD comparison of Co-CAT/CC and RuCo-CAT/CC with simulated Co-CAT pattern.

Geometry: nanorod arrays on carbon cloth
Context: target_sample_vs_pristine_control
Measurement source: article p.2 · Results and Discussion · Figure 1b

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
M-CAT c-direction XRD reflection	27.7 degrees 2theta	—	—	Text Rounded Reported	article p.2 · Results and Discussion · Figure 1b
M-CAT (100) XRD peak	4.6 degrees 2theta	—	—	Text Rounded Reported	article p.2 · Results and Discussion · Figure 1b