Other — Semiconducting Manganese-Bipyridyl Coordination Polymer via a Manganese-Metal-Nanoparticle Approach

Measurement evidence

Other

Semiconducting Manganese-Bipyridyl Coordination Polymer via a Manganese-Metal-Nanoparticle Approach · Reiss A., Gottlicher J., Vitova T. et al. · Inorganic Chemistry · 2025 · 9469-9476

1 measurement group · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetry and XRD of thermal remnant

X-ray diffraction and scattering Thermogravimetric analysis

Manually separated/rinsed crystals of 1 · Single Crystal

Crystals of 1 manually separated and rinsed with toluene; TG measured under dried air up to 1200 deg C at 5 K/min in corundum crucible; XRD used to identify remnant.

Atmosphere: dried air
Geometry: corundum crucible
Context: Purified coordination-polymer crystals
Measurement source: S3,S8 · Differential thermal analysis and thermogravimetry; Characterization · Figure S3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Second TG mass loss	19 % at 560-980 deg C	—	temperature range 560-980 deg C	Text Range	S8 · Characterization · Figure S3a
First TG mass loss	70 % at 80-380 deg C	—	temperature range 80-380 deg C	Text Range	S8 · Characterization · Figure S3a
TG residue identified as MnO	11 % residue, identified by XRD as MnO	—	—	Text Exact Reported	S8 · Characterization · Figure S3