Complete recipeSource: Both
Route 1: Other
text-only SI · 1.2 Synthesized of Co-MOFs
Metal precursors0.1 mmol Co(OAc)2.4H2O
Linker precursors0.05 mmol H2BDC
Solvents35 mL mixed solvent (31 mL DMF, 2 mL methanol and 2 mL water)
Additives100 mg PVP; 0.8 mL triethylamine
Atmospherenot reported
Temperatureultrasonic bath; temperature not reported; water changed every 2 h to prevent temperature rise
Time8
Work-upcentrifuged and washed with DMF reagent and methanol, respectively
Activationvacuum dried at 80 C for 10 h
Scalability context57% yield based on H2BDC
Show 5 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | Co(OAc)2.4H2O | 0.1 mmol | text-only SI · 1.2 Synthesized of Co-MOFs |
| Linker | H2BDC / 1,4-benzenedicarboxylic acid | 0.05 mmol | text-only SI · 1.2 Synthesized of Co-MOFs |
| Solvent | 35 mL mixed solvent (31 mL DMF, 2 mL methanol and 2 mL water) | 35 mL | text-only SI · 1.2 Synthesized of Co-MOFs |
| Additive | poly(vinylpyrrolidone) (PVP) | 100 mg PVP | text-only SI · 1.2 Synthesized of Co-MOFs |
| Base | triethylamine | 0.8 mL | text-only SI · 1.2 Synthesized of Co-MOFs |