Diffraction Structure — Enhancing One-Dimensional Charge Transport in Metal-organic Framework Hexagonal Nanorods for Electrocatalytic Oxygen Evolution

5 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Fe-HXR hexagonal nanorods · Powder

PXRD pattern of Fe-HXR using Cu Kalpha radiation.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Fe-HXR XRD pattern	XRD pattern of Fe-HXR shown with low-angle peaks near 7-10 degrees 2theta	—	—	Caption Qualitative	SI p. 5 · Figure S2 · Figure S2

NiFe-HXR hexagonal nanorods · Powder

PXRD pattern comparison of as-prepared Ni-HXR, Fe-HXR and NiFe-HXR against simulated pattern.

Context: mixed-metal pristine framework
Measurement source: 1831 · Results and discussion · Figure 1f and Figure S2 referenced

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
PXRD phase match	as-prepared Ni-HXR, Fe-HXR and NiFe-HXR match the simulated pattern	—	—	Text Qualitative	1831 · Results and discussion · Figure 1f and Figure S2 referenced

NiFe-HXR hexagonal nanorods · Powder

PXRD before/after OER stability measurement.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
post-stability XRD structure retention	maintains initial crystalline structure after chronoamperometry	—	—	Text Qualitative	1833 · Electrocatalytic properties · Figure S9

NiFeOx derived oxide · Powder

PXRD pattern of derived NiFeOx.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
NiFeOx XRD assignment	NiFeOx with NiO reflections marked in Figure S3	—	—	Caption Qualitative	SI p. 6 · Figure S3 · Figure S3

Ni-HXR hexagonal nanorods · Powder

Crystal structure determination of Ni-HXR.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ni-HXR space group	C2/c	—	—	Text Exact Reported	1831 · Results and discussion · Figure 1
cofacial terminal-ligand pi-pi stacking distance	about 3.7 A	—	—	Text Approximate	1831 · Results and discussion · Figure 1d