Diffraction Structure — Guest-Assisted Proton Conduction in the Sulfonic Mesoporous MIL-101 MOF

Measurement evidence

Diffraction Structure

Guest-Assisted Proton Conduction in the Sulfonic Mesoporous MIL-101 MOF · Devautour-Vinot S., Sanil E.S., Geneste A. et al. · Chemistry - An Asian Journal · 2019 · 3561-3565

4 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

XRPD

H2SO4(1M)@MIL-101(Cr)-NH-(CH2)3SO3H powder · Powder

Before and after conductivity measurements.

Temperature
298
Atmosphere
ambient
Geometry
powder
Context
guest-loaded target
Measurement source
4 · Results · Figure 1a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Framework retained after H2SO4 loadinggood agreement between XRPD patterns of H2SO4-loaded solids and guest-free materialText
Qualitative
4 · Results · Figure 1a

XRPD

MIL-101(Cr)-NO2 powder · Powder

Powder X-ray diffraction compared with MIL-101(Cr) pattern.

Temperature
298
Atmosphere
ambient
Geometry
powder
Context
parent precursor
Measurement source
2 · Results · Figure 1a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
XRPD phase matchmatches MIL-101(Cr)Text
Qualitative
2 · Results · Figure 1a

XRPD

MIL-101(Cr)-NH-(CH2)3SO3H powder · Powder

Before and after conductivity measurements.

Temperature
298
Atmosphere
ambient
Geometry
powder
Context
guest-free target
Measurement source
3 · Results · Figure 1a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Framework retained after PSM and conductivityframework integrity is retained after PSM; pattern remains similar after conductivityText
Qualitative
2-3 · Results · Figure 1a

XRPD

Washed H2SO4(1M)@MIL-101(Cr)-NH-(CH2)3SO3H powder · Powder

Washed H2SO4-loaded sample after conductivity measurements.

Temperature
298
Atmosphere
ambient
Geometry
powder
Context
recovered guest-free sample
Measurement source
5 · Results · Figure 1a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Washed sample XRPD recoverygood agreement between washed and parent XRPD patternsText
Qualitative
5 · Results · Figure 1a