Diffraction Structure — Nanocubic bimetallic organic framework self-templated from Ni precursor as efficient electrocatalysts for oxygen evolution reaction

Measurement evidence

Diffraction Structure

Nanocubic bimetallic organic framework self-templated from Ni precursor as efficient electrocatalysts for oxygen evolution reaction · Yuan B., Li C., Liu Y. et al. · International Journal of Hydrogen Energy · 2019 · 11705-11716

2 measurement groups · 2 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Powder X-ray diffraction

X-ray diffraction and scattering

MIL-53(Fe) · Powder

XRD pattern compared with simulated/reported MIL-53(Fe).

Geometry: powder
Context: pristine MOF control
Measurement source: 11708 · Morphology and structure characterization · Fig. S6

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source

Powder X-ray diffraction (Cu Kalpha)

X-ray diffraction and scattering

Ni NCs@MIL-53(NiFe), optimised Ni NCs:FeCl2 mass ratio 3 · Powder

Bruker D8 Advance powder diffractometer, Cu Kalpha radiation, lambda = 1.5418 A.

Geometry: powder
Context: target mixed-metal/composite MOF
Measurement source: 11707 · Structural characterizations · Fig. 2a

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
MIL-53-related XRD peak	8.86 deg, assigned to (200) crystal plane of MIL-53 structure	—	—	Text Exact Reported	11708 · Morphology and structure characterization · Fig. 2a
Target phase assignment	mixed crystalline structure of MIL-53(NiFe) and tetragonal acetate hydroxide phase	—	—	Qualitative Qualitative	11708 · Morphology and structure characterization · Fig. 2a