Microscopy Morphology — Conductive MOF-Modified Separator for Mitigating the Shuttle Effect of Lithium-Sulfur Battery through a Filtration Method

Measurement evidence

Microscopy Morphology

Conductive MOF-Modified Separator for Mitigating the Shuttle Effect of Lithium-Sulfur Battery through a Filtration Method · Chen H., Xiao Y., Chen C. et al. · ACS Applied Materials and Interfaces · 2019 · 11459-11465

3 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM elemental mapping

Ni3(HITP)2 after Li-S cell cycling/discharge · Powder

Elemental mapping of Ni3(HITP)2 before and after cycling.

Geometry
powder recovered from cycling
Context
post-cycling MOF
Measurement source
main p.3, article p.11461 · Results and Discussion · Fig. S5; Fig. S6
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Sulfur detected on cycled Ni3(HITP)2After cycling, elemental mapping shows sulfur on Ni3(HITP)2.Text
Qualitative
main p.3, article p.11461 · Results and Discussion · Fig. S5; Fig. S6

Cross-sectional and top-view SEM

Ni3(HITP)2-modified separator · Thin Film

SEM of Ni3(HITP)2 layer stacked on PP surface.

Geometry
coated separator cross-section and surface
Context
composite separator
Measurement source
main p.3, article p.11461 · Results and Discussion · Fig. 1c,d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Ni3(HITP)2 layer thickness on PP8 umText
Rounded Reported
main p.3, article p.11461 · Results and Discussion · Fig. 1c
Top-view modified separator morphologyTop-view SEM of the Ni3(HITP)2 layer on separator shows thornlike morphology.Text
Qualitative
main p.3, article p.11461 · Results and Discussion · Fig. 1d

SEM and TEM

As-synthesised Ni3(HITP)2 powder · Powder

Low- and high-magnification images of synthesised Ni3(HITP)2 powder.

Context
pristine MOF powder
Measurement source
SI p.S-3 · Supporting Information · Fig. S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Pristine Ni3(HITP)2 morphologyAggregated crystals with thornlike morphology and rough surface.Text
Qualitative
main p.2, article p.11460 · Results and Discussion · Fig. S2a-d