Microscopy Morphology — Enhancing the energy storage performances of metal-organic frameworks by controlling microstructure

3 measurement groups · 9 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

A-CuHHTP powder · Powder

SEM at 5 kV after Pt sputter coating; TEM at 200 keV with low beam flux.

Geometry: powder particles on SEM/TEM supports
Context: pristine powder
Measurement source: p003-p004 / journal p9212-p9213 · Results & discussion · Fig. 3; SI Fig. S1-S2; Table S2

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
A-CuHHTP length-to-width aspect ratio upper bound	length-to-width aspect ratio 0.01-0.23	—	range	Text Range	p003 / journal p9212 · Results & discussion · Table S2
A-CuHHTP length-to-width aspect ratio lower boundMarked as a best value within this paper	length-to-width aspect ratio 0.01-0.23	—	range	Text Range	p003 / journal p9212 · Results & discussion · Table S2
A-CuHHTP flake diameter upper bound	flake diameters 0.5-2.9 um	—	range	Text Range	p003 / journal p9212 · Results & discussion · Fig. 3a; SI Fig. S1
A-CuHHTP flake diameter lower bound	flake diameters 0.5-2.9 um	—	range	Text Range	p003 / journal p9212 · Results & discussion · Fig. 3a; SI Fig. S1

B-CuHHTP powder · Powder

SEM at 5 kV after Pt sputter coating; TEM at 200 keV with low beam flux; FFT/line profile analysis.

Geometry: powder particles on SEM/TEM supports
Context: pristine powder
Measurement source: p003-p004 / journal p9212-p9213 · Results & discussion · Fig. 3; SI Fig. S3-S4; Table S3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
B-CuHHTP length-to-width aspect ratio upper bound	length-to-width aspect ratio 1-37	—	range	Text Range	p003 / journal p9212 · Results & discussion · Table S3
B-CuHHTP length-to-width aspect ratio lower bound	length-to-width aspect ratio 1-37	—	range	Text Range	p003 / journal p9212 · Results & discussion · Table S3
B-CuHHTP rod length upper bound	rod lengths 0.5-4 um	—	range	Text Range	p003 / journal p9212 · Results & discussion · Fig. 3c; SI Fig. S3
B-CuHHTP rod length lower bound	rod lengths 0.5-4 um	—	range	Text Range	p003 / journal p9212 · Results & discussion · Fig. 3c; SI Fig. S3

C-CuHHTP powder · Powder

SEM at 5 kV after Pt sputter coating; TEM not able to examine pore network because agglomerates were thick.

Geometry: powder particles on SEM support
Context: pristine powder
Measurement source: p003-p004 / journal p9212-p9213 · Results & discussion · Fig. 3e

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
C-CuHHTP agglomerate cluster size	ca. 0.5-1 um spherical clusters	—	range lower bound	Text Approximate	p003 / journal p9212 · Results & discussion · Fig. 3e