Microscopy Morphology — Stabilization of Hexaaminobenzene in a 2D Conductive Metal-Organic Framework for High Power Sodium Storage

Measurement evidence

Microscopy Morphology

Stabilization of Hexaaminobenzene in a 2D Conductive Metal-Organic Framework for High Power Sodium Storage · Park J., Lee M., Feng D. et al. · Journal of the American Chemical Society · 2018 · 10315-10323

1 measurement group · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

HRTEM, TEM and SEM

Scanning electron microscopy Transmission electron microscopy

Co-HAB-D optimised mixed-solvent product · Powder

TEM samples dispersed in acetone and transferred to carbon-coated copper grid; JEOL JEM2100 at 200 kV under low dose; SEM at 5-10 kV.

Temperature: about 300
Atmosphere: TEM/SEM vacuum
Geometry: powder crystallites on microscopy grids/stubs
Context: pristine framework
Measurement source: SI p.S7 · Transmission electron microscopic (TEM) analysis · Fig. 1d; Fig. 2a,b

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co-HAB-D crystallite long-side size	~75 nm on the long side	—	—	Text Approximate	main p.10318 · Results and Discussion · Fig. 2a,b
HRTEM d100 spacing	d100 = 1.17 nm	—	—	Text Rounded Reported	SI p.S7 · TEM analysis · Fig. 1d
Hexagonal pores observed	hexagonal pores smaller than 1 nm; honeycomb arrangement along [001]	—	—	Qualitative Qualitative	main p.10317 · Results and Discussion · Fig. 1d
HRTEM pore diameter	~0.7 nm	—	—	Text Approximate	SI p.S7 · TEM analysis · Fig. 1d