Other — Mn2(2,5-disulfhydrylbenzene-1,4-dicarboxylate): A microporous metal-organic framework with infinite (-Mn-S-)∞ chains and high intrinsic charge mobility

Measurement evidence

Other

Mn2(2,5-disulfhydrylbenzene-1,4-dicarboxylate): A microporous metal-organic framework with infinite (-Mn-S-)∞ chains and high intrinsic charge mobility · Sun L., Miyakai T., Seki S. et al. · Journal of the American Chemical Society · 2013 · 8185-8188

2 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetric analysis

As-synthesized 1 powder · Powder

TA Instruments Q500, 2 deg C/min under N2 flow of 90 mL/min.

Atmosphere
nitrogen
Context
Guest-loaded as-synthesized framework
Measurement source
SI p.S2 · Physical characterizations · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
As-synthesized absorbed DMF loss annotation31.83% absorbed DMF lossVisual Estimate
Rounded Reported
SI p.S8 · Figure S1 · Figure S1
As-synthesized TGA mass lossMarked as a best value within this paper31.8% between 50 and 365 deg CText
Rounded Reported
main p.8186 · Main text, TGA · Figure S1

Thermogravimetric analysis

Methanol-exchanged 1 powder · Powder

TA Instruments Q500, 2 deg C/min under N2 flow; held at 100 deg C and 150 deg C for 30 min.

Atmosphere
nitrogen
Context
Methanol-exchanged framework
Measurement source
SI p.S9 · Figure S2 caption · Figure S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Methanol-exchanged absorbed MeOH loss annotationMarked as a best value within this paper26.73% absorbed MeOH lossVisual Estimate
Rounded Reported
SI p.S9 · Figure S2 · Figure S2
Methanol-exchanged stable TGA plateaustable plateau between 150 and 400 deg Crange 150-400 deg CText
Range
main p.8187 · Main text, activation · Figure S2