Thermogravimetric analysis (TA TGA-55)
As-synthesised Cu3(HHTP)2 dark-blue crystalline solid · Powder
SI reports heating rate as 50C/min in N2 environment; thermal stability and solvent loss assessed.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Approximate residual weight at high temperature | about 45 wt% remaining near 850 C from Supplementary Fig. 2 | 45 wt% | visual estimate from rendered TGA curve; about +/-3 wt% | Visual Estimate Approximate | SI rendered p.3 · Thermal gravimetric analysis (TGA) · Supplementary Fig. 2 |
| Thermal stability upper temperature | No prominent loss after till 8500C; interpreted as up to 850 C | 1123.15 K | OCR-like SI temperature formatting | Text Uncertain | SI text p.1 · Thermal gravimetric analysis (TGA) · Supplementary Fig. 2 |
| TGA NMP solvent-loss temperature range | 1850C -2850C in SI text, interpreted as 185-285 C | 508.15 K | range 185-285 C; OCR-like SI temperature formatting | Text Uncertain | SI text p.1 · Thermal gravimetric analysis (TGA) · Supplementary Fig. 2 |