Microscopy Morphology — Trimetallic conductive metal-organic frameworks as precatalysts for the oxygen evolution reaction with enhanced activity

4 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FeCo0.6Ni0.4-CAT powder/electrode, Fe/(Co+Ni) about 0.32 · Electrode

Elemental mapping for Co, Ni and Fe in FeCo0.6Ni0.4-CAT nanorods.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Co/Ni/Fe distribution	Co, Ni, and Fe homogeneously distributed in FeCo0.6Ni0.4-CAT nanorods	—	—	Qualitative Qualitative	3 · Results and discussion · Fig. 1e

FeCo0.6Ni0.4-CAT powder/electrode, Fe/(Co+Ni) about 0.32 · Electrode

FEI Tecnai F20 TEM with EDX, accelerating voltage 200 kV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Lattice fringe spacing	1.91 nm	—	—	Text Exact Reported	3 · Results and discussion · Fig. 1d

Co0.6Ni0.4-CAT powder/electrode · Electrode

Zeiss Supra 55 SEM, accelerating voltage 5 kV.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Average nanorod diameter	70 nm	—	—	Text Rounded Reported	3 · Results and discussion · Fig. 1b-c

FeCo0.8Ni0.2-CAT powder/electrode · Electrode

SI SEM images compare Co-CAT, FeCo-CAT, Ni-CAT, FeNi-CAT, Co0.8Ni0.2-CAT, FeCo0.8Ni0.2-CAT, Co0.4Ni0.6-CAT and FeCo0.4Ni0.6-CAT.

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
SEM morphology comparison across Co/Ni and Fe-exchanged variants	SEM images show rod-like particles for the listed M-CAT variants	—	—	Visual Estimate Qualitative	S-3 · Supporting Information · Figure S2