Diffraction Structure — Conductive metal–Organic frameworks endow high-efficient oxygen evolution of La0·6Sr0·4Co0·8Fe0·2O3 perovskite oxide nanofibers

Measurement evidence

Diffraction Structure

Conductive metal–Organic frameworks endow high-efficient oxygen evolution of La0·6Sr0·4Co0·8Fe0·2O3 perovskite oxide nanofibers · Li Z., Li J.-G., Ao X. et al. · Electrochimica Acta · 2020 · 135638

2 measurement groups · 3 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Supplementary XRD pattern comparison

LSCF@Ni3(HITP)2-2 · Powder

Rendered SI Fig. S1 compares as-prepared LSCF, bare Ni3(HITP)2 and LSCF@Ni3(HITP)2-1/-2/-3/-4.

Context
Pristine LSCF, bare conductive MOF and four composite variants.
Measurement source
2 · Supporting Information · Fig. S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
XRD loading series retains LSCF peaksLSCF@Ni3(HITP)2-1/-2/-3/-4 retain the LSCF peak pattern while the Ni3(HITP)2 trace is broad/featureless in the rendered SI comparison.Visual Estimate
Qualitative
2 · Supporting Information · Fig. S1

Powder X-ray diffraction (XRD)

LSCF NFs · Powder

Philips X'pert Pro, Cu Kalpha lambda 1.5406 A, 40 kV, 40 mA, room temperature; LSCF, Ni3(HITP)2 and LSCF@Ni3(HITP)2-2 compared.

Temperature
room temperature
Context
Pristine LSCF and composite comparison.
Measurement source
2 · 2.4 Material characterizations · Fig. 2a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
LSCF XRD peak positions23.1, 33.0, 40.6, 47.3, 53.4, 58.7, 69.3, 73.9 and 78.8 deg 2thetaText
Rounded Reported
3 · Results and discussion · Fig. 2a
Ni3(HITP)2 XRD crystallinity in compositeNo additional peaks after Ni3(HITP)2 growth; described as amorphous or below XRD detection limit.Qualitative
Qualitative
3 · Results and discussion · Fig. 2a and Fig. S1