X-ray photoelectron spectroscopy (XPS)
LSCF@Ni3(HITP)2-2 · Powder
Kratos AXIS Ultra DLD-600 W using Al Kalpha 1486.6 eV source; C 1s at 284.8 eV used as reference.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Co 2p3/2 positive binding-energy shift versus LSCF | 0.7 eV | — | — | Text Rounded Reported | 5 · Results and discussion · Fig. 3a |
| Fe 2p3/2 positive binding-energy shift versus LSCF | 0.5 eV | — | — | Text Rounded Reported | 5 · Results and discussion · Fig. 3b |
| Ni3+ 2p3/2 binding energy | 854.9 eV | — | — | Text Rounded Reported | 5 · Results and discussion · Fig. 3c |
| O 1s lattice oxygen peak | 528.9 eV | — | — | Text Rounded Reported | 5 · Results and discussion · Fig. 3d |
| O 1s superoxidative oxygen peak | 530.6 eV | — | — | Text Rounded Reported | 5 · Results and discussion · Fig. 3d |