Thermogravimetric analysis on PerkinElmer Pyris Diamond TG/DTA
As-synthesised bulk compound 1 powder/crystals · Powder
30-600 deg C under nitrogen, flow rate 50 cm3 min-1, heating rate 2 deg C/min.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| First TGA weight loss | 2.08% observed; 2.51% calculated | — | — | Text Exact Reported | 767 · Thermal Stability and Purity · Figure S4 |
| Calculated lattice-water weight loss | 2.51% calculated | — | — | Text Exact Reported | 767 · Thermal Stability and Purity · Figure S4 |
| TGA first loss upper temperature | 125 deg C | — | — | Text Exact Reported | 767 · Thermal Stability and Purity · Figure S4 |
| TGA first loss lower temperature | 80 deg C | — | — | Text Exact Reported | 767 · Thermal Stability and Purity · Figure S4 |
| Thermal stability limit before decomposition | stable up to 250 deg C; starts decomposing after 250 deg C | — | — | Text Rounded Reported | 767 · Thermal Stability and Purity · Figure S4 |