Other — An Electrically Conducting Li-Ion Metal-Organic Framework

Measurement evidence

Other

An Electrically Conducting Li-Ion Metal-Organic Framework · Rambabu D., Lakraychi A.E., Wang J. et al. · Journal of the American Chemical Society · 2021 · 11641-11650

3 measurement groups · 4 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

ICP-AES

Li2-Mn-DOBDC powder · Powder

Metal ratios Mg or Mn:Li analysed with ICAP 6500 instrument.

Geometry
powder digestion not specified
Context
pristine lithiated powders
Measurement source
4 · 2.1. Synthesis, Structural Reversibility, and Physicochemical Analysis
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Li2-Mg-DOBDC Mg:Li ratio1:1.89 (Mg:Li)1.89 Li/MgText
Exact Reported
4 · 2.1
Li2-Mn-DOBDC Mn:Li ratio1:1.94 (Mn:Li)1.94 Li/MnText
Exact Reported
4 · 2.1

thermogravimetric analysis (TGA)

Li2-Mg-DOBDC powder · Powder

Under argon, heating rate 10 degC/min between 25 and 800 degC.

Atmosphere
argon
Geometry
powder
Context
pristine Mg-series powders
Measurement source
19 · Supplementary Figures and Data · Figure S5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource

thermogravimetric analysis (TGA)

Li2-Mn-DOBDC powder · Powder

Under argon, heating rate 10 degC/min between 25 and 800 degC.

Atmosphere
argon
Geometry
powder
Context
pristine Mn-series powders
Measurement source
6,15 · 1.3 Instrumentation; Figure S2 · Figure S2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
H2-Mn-DOBDC approximate stability before decomposition~250 degC followed by a weight loss at ~500 degC523.15 K~Text
Approximate
15 · Figure S2 discussion · Figure S2
Li2-Mn-DOBDC thermal stability with no significant mass lossMarked as a best value within this paperno significant mass loss up to ~550 degC823.15 K~Text
Approximate
15 · Figure S2 discussion · Figure S2