Microscopy Morphology — Highly Conductive Bimetallic Ni-Fe Metal Organic Framework as a Novel Electrocatalyst for Water Oxidation

Measurement evidence

Microscopy Morphology

Highly Conductive Bimetallic Ni-Fe Metal Organic Framework as a Novel Electrocatalyst for Water Oxidation · Zheng F., Xiang D., Li P. et al. · ACS Sustainable Chemistry and Engineering · 2019 · 9743-9749

1 measurement group · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM, TEM, HAADF-STEM and STEM-EDS mapping

Scanning electron microscopy Transmission electron microscopy Elemental microanalysis and mapping

FeNi-DOBDC-3 · Nanosheet

SEM at 30 kV; HRTEM at 200 kV; samples dispersed from ethanol onto silicon wafer or carbon-coated copper TEM grids.

Atmosphere: ambient drying for microscopy sample preparation
Context: Pristine FeNi-DOBDC nanosheet samples and controls.
Measurement source: p003-p005 / article pp.9745-9747 · Results and Discussion · Figure 2; Figure S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Elemental distribution in FeNi-DOBDC-3	Fe, Ni, C, O and S elements have highly uniform distributions	—	—	Text Qualitative	p005 / article p.9747 · Results and Discussion · Figure 2e,f
FeNi-DOBDC-1 mean nanosheet thickness	18.3 nm	—	—	Figure Axis Rounded Reported	p010 / S10 · Figure S5 · Figure S5e
FeNi-DOBDC-2 mean nanosheet thickness	18.5 nm	—	—	Figure Axis Rounded Reported	p010 / S10 · Figure S5 · Figure S5f
FeNi-DOBDC-3 mean nanosheet thickness	19.0 nm	—	—	Figure Axis Rounded Reported	p010 / S10 · Figure S5 · Figure S5g
FeNi-DOBDC-4 mean nanosheet thickness	33.4 nm	—	—	Figure Axis Rounded Reported	p010 / S10 · Figure S5 · Figure S5h