Thermogravimetric analysis (TGA)
Ni3(HATI_H)2 black powder · Powder
Under N2 atmosphere, heating rate 5 C min-1; supercritical CO2 drying 4 h, 90 C overnight activation and in-situ activation 100 C for 1 h.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| decomposition onset | above 200 C | — | — | Caption Approximate | p015 · Supplementary Figures · Figure S4 |
| desolvation onset | over 100 C | — | — | Text Approximate | p002 · Synthesis and Characterization · Figure S4 |