Microscopy Morphology — Nanorods of a novel highly conductive 2D metal-organic framework based on perthiolated coronene for thermoelectric conversion

Measurement evidence

Microscopy Morphology

Nanorods of a novel highly conductive 2D metal-organic framework based on perthiolated coronene for thermoelectric conversion · Chen Z., Cui Y., Jin Y. et al. · Journal of Materials Chemistry C · 2020 · 8199-8205

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Scanning electron microscopy (SEM)

Scanning electron microscopy

Ni-PTC nanorod dark powder · Powder

Hitachi S4800-SEM at 5 kV; samples on conductive silicon substrates and coated with platinum thin film.

Geometry: nanorods
Context: pristine Ni-PTC MOF powder
Measurement source: 3 · Synthesis and structural characterizations · Fig. S4

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Nanorod length upper bound	500 nm to 5 um length	5 um	range	Text Range	3 · Synthesis and structural characterizations · Fig. S4
Nanorod length lower bound	500 nm to 5 um length	0.5 um	range	Text Range	3 · Synthesis and structural characterizations · Fig. S4
Nanorod width range	50 nm to more than 200 nm in width	—	50 to >200 nm	Text Range	3 · Synthesis and structural characterizations · Fig. S4

TEM, HRTEM, SAED and FFT

Transmission electron microscopy

Ni-PTC nanorod dark powder · Powder

JEOL 2100F TEM with 120 kV acceleration voltage.

Geometry: nanorods
Context: pristine Ni-PTC MOF powder
Measurement source: 3 · Synthesis and structural characterizations · Fig. 2c-f; Fig. S5

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
In-plane honeycomb d-space	d-space = 11.8 A	—	—	Text Rounded Reported	3 · Synthesis and structural characterizations · Fig. 2d
Interlayer distance	about 3.4 A	—	—	Text Approximate	3 · Synthesis and structural characterizations · Fig. 2e; Fig. S3c