Measurement evidence
Field effect transistor based on proton conductive metal organic framework (CuBTC) · Bodkhe G.A., Deshmukh M.A., Patil H.K. et al. · Journal of Physics D: Applied Physics · 2019 · 335105
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Im@CuBTC powder/crystals · Powder
Elemental analysis of CuBTC and Im@CuBTC.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Nitrogen detected in Im@CuBTC by EDS | nitrogen present in Im@CuBTC | — | — | Qualitative Qualitative | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 4 |
Im@CuBTC powder/crystals · Powder
4000-500 cm^-1; comparison of as-synthesised CuBTC and Im@CuBTC.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| CuBTC FTIR carboxylic-acid related band | 1373 cm^-1 | — | — | Text Exact Reported | rendered page 6 / article p. 5 · 3. Results and discussion · Figure 1 |
| CuBTC FTIR carboxylate/C=C band | 1446 cm^-1 | — | — | Text Exact Reported | rendered page 6 / article p. 5 · 3. Results and discussion · Figure 1 |
| CuBTC FTIR C-H asymmetric stretch | 2890 cm^-1 | — | — | Text Exact Reported | rendered page 6 / article p. 5 · 3. Results and discussion · Figure 1 |
| CuBTC FTIR Cu-O stretch | about 730 cm^-1 | — | — | Text Approximate | rendered page 6 / article p. 5 · 3. Results and discussion · Figure 1 |
| Im@CuBTC FTIR amine C-N stretch | 1066 cm^-1 | — | — | Text Exact Reported | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 1 |
| Im@CuBTC FTIR aromatic amine C-N stretch | 1266 cm^-1 | — | — | Text Exact Reported | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 1 |
| Im@CuBTC FTIR aromatic amine C-N stretch | 1324 cm^-1 | — | — | Text Exact Reported | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 1 |
| Im@CuBTC FTIR amine C-N stretch | 1644 cm^-1 | — | — | Text Exact Reported | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 1 |
Im@CuBTC powder/crystals · Powder
Room-temperature C K-edge, O K-edge, N K-edge and Cu L-edge spectra at Indus-2 BL-01.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu, C and O edge XANES similarity after loading | Cu L-edge, C K-edge and O K-edge spectra similar for CuBTC and Im@CuBTC | — | — | Qualitative Qualitative | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 6 |
| N K-edge imidazole features in Im@CuBTC | features related to imidazole observed only for Im@CuBTC | — | — | Qualitative Qualitative | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 6(B) |
Im@CuBTC powder/crystals · Powder
Survey and high-resolution N 1s, Cu 2p and O 1s spectra for CuBTC and Im@CuBTC; Cu-holder background recorded.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| Cu 2p3/2 XPS peak | 937.9 eV | — | — | Text Exact Reported | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 5(C) |
| Cu 2p1/2 XPS peak | 957.87 eV | — | — | Text Exact Reported | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 5(C) |
| Im@CuBTC XPS N 1s peak | N 1s observed; figure labels 404.85 eV | — | — | Figure Axis Rounded Reported | rendered page 5 / article p. 4 · 3. Results and discussion · Figure 5(B) |
| O 1s carboxylic species peak | 531.1 eV | — | — | Text Exact Reported | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 5(D) |
| O 1s Cu2(O2CR)4 group peak | 535.91 eV | — | — | Text Exact Reported | rendered page 7 / article p. 6 · 3. Results and discussion · Figure 5(D) |