Diffraction Structure — Mixed-metallic MOF based electrode materials for high performance hybrid supercapacitors

Measurement evidence

Diffraction Structure

Mixed-metallic MOF based electrode materials for high performance hybrid supercapacitors · Jiao Y., Pei J., Chen D. et al. · Journal of Materials Chemistry A · 2017 · 1094-1102

4 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Post-cycling XRD and SEM

Co/Ni-MOF NAFLs · Nanosheet

XRD after 3000 and 5000 cycles; SEM after 5000 cycles; compared with Zn/Ni-MOF and Ni-MOF.

Context
cycled MOF electrodes
Measurement source
p008 / 1101 · Results and discussion · Fig. 9
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
M-MOF diffraction after 5000 cyclesMarked as a best value within this paperall diffraction peaks of the M-MOFs still existText
Qualitative
p007 / 1100 · Results and discussion · Fig. 9a,b
Ni-MOF diffraction after 5000 cyclesdiffraction peaks of the Ni-MOF disappearedText
Qualitative
p007 / 1100 · Results and discussion · Fig. 9b

Powder XRD with Cu-Kalpha radiation

Co/Ni-MOF NAFLs · Nanosheet

Isostructural comparison with Ni-MOF simulated pattern.

Context
mixed-metal pristine framework
Measurement source
p003 / 1096 · Results and discussion · Fig. 3a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
XRD phase/topology assignmentall patterns show evident similarity; same layered topology crystal structureText
Qualitative
p003 / 1096 · Results and discussion · Fig. 3a,b

Powder XRD with Cu-Kalpha radiation

Ni-MOF powder / NAFL control · Nanosheet

Compared with simulated pattern from [Ni3(OH)2(C8H4O4)2(H2O)4].2H2O (CCDC 638866).

Context
pristine control
Measurement source
p003 / 1096 · Results and discussion · Fig. 3a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Layer interspaceabout 0.95 nmText
Approximate
p003 / 1096 · Results and discussion · Fig. 3c-e

Powder XRD with Cu-Kalpha radiation

Zn/Ni-MOF NAFLs · Nanosheet

Isostructural comparison with Ni-MOF simulated pattern.

Context
mixed-metal pristine framework
Measurement source
p003 / 1096 · Results and discussion · Fig. 3a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Layer interspace after Zn substitutionMarked as a best value within this paperfrom 0.95 nm to 1.04 nmText
Approximate
p006 / 1099 · Results and discussion