Measurement evidence
Paramagnetic Conducting Metal–Organic Frameworks with Three-Dimensional Structure · Wu X., Qiu Y., Chen Z. et al. · Angewandte Chemie - International Edition · 2020 · 20873-20878
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
Co-THBQ well-crystallised powder · Powder
TEM/HRTEM used JEM 2100F at 120 kV after ethanol dispersion and deposition on a carbon-coated copper grid.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| HRTEM lattice spacing | 10.8 A | — | — | Text Rounded Reported | 3 · Morphological structures · Figure 3h |
| SEM morphology | regular octahedron geometry with scale of several tens of nanometers | — | — | Text Qualitative | 2 · Morphological structures · Figure 3b |
Fe-THBQ black powder · Powder
TEM/HRTEM used JEM 2100F at 120 kV; about 2 mg framework dispersed in 4 ml waterless ethanol by 5 min ultrasonication and dropped on carbon-coated copper grid.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| HRTEM lattice fringe spacing | 10.6 A | — | — | Text Rounded Reported | 3 · Morphological structures · Figure 3g |
| SEM morphology | compact hexagon sheet morphology with side length around 50 nm | — | around | Text Approximate | 2 · Morphological structures · Figure 3a |
Mn-THBQ powder · Powder
TEM/HRTEM used JEM 2100F at 120 kV after ethanol dispersion and deposition on a carbon-coated copper grid.
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| HRTEM lattice spacing | 5.5 A | — | — | Text Rounded Reported | 3 · Morphological structures · Figure 3i |
| SEM morphology | nanosheet morphology with thickness of 5 nm | — | — | Text Rounded Reported | 2 · Morphological structures · Figure 3c |