Microscopy Morphology — Solid-State Electrochemical Carbon Dioxide Capture by Conductive Metal-Organic Framework Incorporating Nickel Bis(diimine) Units

Measurement evidence

Microscopy Morphology

Solid-State Electrochemical Carbon Dioxide Capture by Conductive Metal-Organic Framework Incorporating Nickel Bis(diimine) Units · Liu J., Yang M., Zhou X. et al. · Journal of the American Chemical Society · 2024 · 33093-33103

2 measurement groups · 1 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM before and after CO2 capture/release cycling

Ni3(HITP)2 recovered after capture-release cycling · Powder

Recovered MOF after cycling compared with pre-test morphology.

Context
post-cycling framework stability
Measurement source
S28 · 11. Electrode Materials Before and After Test · Figure S31
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
SEM morphology after capture-release cyclingsimilar morphology to before cyclingQualitative
Qualitative
33097 · Evaluation of the eCC Performance of the MOF Ni3(HITP)2 · Figure S31

Scanning electron microscopy

As-synthesised Ni3(HITP)2 dark-blue powder · Powder

ZEISS GeminiSEM 450; material pressed onto carbon conductive tape; 8 mm working distance; 20 kV beamline; 10^-4 torr vacuum.

Atmosphere
vacuum
Geometry
Powder on carbon tape/aluminium plate
Context
pristine framework powder
Measurement source
S10 · 5. Scanning Electron Microscopy · Figure S8
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource