Complete recipeSource: Both
Route 1: Hydrothermal
S1 · Synthesis of (NH4)2(adp)[Zn2(ox)3].3H2O
Metal precursorsZnO (10 mmol, 814 mg)
Linker precursorsH2(ox).2H2O (20 mmol, 2521 mg) and adipamide (10 mmol, 1442 mg); adipamide converted to adipic acid under hydrothermal conditions.
Solventsdistilled water (550 mmol, 10 ml)
Atmospherenot specified
Temperature130
Time24
Work-upSlowly cooled to room temperature over 168 h; precipitate collected by filtration and washed with distilled water.
ActivationAir-dried; no separate activation reported.
Scalability contextYield reported as 2891 mg, 92%.
Show 4 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | ZnO | 10 mmol, 814 mg | S1 · Synthesis of (NH4)2(adp)[Zn2(ox)3].3H2O |
| Linker | H2(ox).2H2O | 20 mmol, 2521 mg | S1 · Synthesis of (NH4)2(adp)[Zn2(ox)3].3H2O |
| Linker | adipamide | 10 mmol, 1442 mg | S1 · Synthesis of (NH4)2(adp)[Zn2(ox)3].3H2O |
| Solvent | distilled water | 550 mmol, 10 ml | S1 · Synthesis of (NH4)2(adp)[Zn2(ox)3].3H2O |