Spectroscopy — Highly sensitive and selective electrochemical sensor for carbendazim detection in fruit juice using novel bi-metallic metal organic framework anchored graphite rod electrode

Measurement evidence

Spectroscopy

Highly sensitive and selective electrochemical sensor for carbendazim detection in fruit juice using novel bi-metallic metal organic framework anchored graphite rod electrode · Dey B., Kushwaha K.S., Ullah I. et al. · Inorganic Chemistry Communications · 2025 · 114643

3 measurement groups · 6 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FTIR spectroscopy

Self-standing Ni-Fe(PDC)/GR electrode · Electrode

PerkinElmer FTIR L1280127, ATR mode, 4000-400 cm^-1; compared pure graphite rod and MOF-deposited graphite rod.

Context
graphite control and MOF/GR composite
Measurement source
2 · 2.3. Characterization equipment · Fig. 1a
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
graphite C=C FTIR peak1532 cm^-1Text
Exact Reported
4 · 3.1. FTIR analysis · Fig. 1a
MOF metal-ligand FTIR peak660 cm^-1Text
Exact Reported
4 · 3.1. FTIR analysis · Fig. 1a

Raman spectroscopy

Self-standing Ni-Fe(PDC)/GR electrode · Electrode

Bruker RFS 27 Raman spectrophotometer with 532 nm Nd:YAG laser; compared pure graphite and MOF-deposited graphite rods.

Context
graphite control and MOF/GR composite
Measurement source
2 · 2.3. Characterization equipment · Fig. 1b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
graphite D-band Raman peak1350 cm^-1Text
Exact Reported
4 · 3.2. Raman spectra analysis · Fig. 1b
MOF carboxylate Raman peak1565 cm^-1Text
Exact Reported
4 · 3.2. Raman spectra analysis · Fig. 1b

X-ray photoelectron spectroscopy

Self-standing Ni-Fe(PDC)/GR electrode · Electrode

Thermo Fisher Scientific K-alpha XPS; high-resolution and survey spectra at pass energies of 0.1 eV and 1 eV.

Context
composite target
Measurement source
2 · 2.3. Characterization equipment · Fig. 2
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Fe 2p3/2 binding energy712.2 eVText
Approximate
4 · 3.5. XPS study · Fig. 2f
Ni 2p3/2 binding energy855.9 eVText
Exact Reported
4 · 3.5. XPS study · Fig. 2e