Microscopy Morphology — Engineering the modulation of the active sites and pores of pristine metal-organic frameworks for high-performance sodium-ion storage

Measurement evidence

Microscopy Morphology

Engineering the modulation of the active sites and pores of pristine metal-organic frameworks for high-performance sodium-ion storage · Shuang W., Wang Y., Chen F. et al. · Inorganic Chemistry Frontiers · 2022 · 396-405

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

FESEM, TEM and HRTEM

Scanning electron microscopy Transmission electron microscopy

Ni-HHTP-250 · Powder

Morphology of pristine and thermally treated powders; HRTEM lattice distance for Ni-HHTP-250.

Context: pristine MOF powder
Measurement source: 399 · Synthesis and characterization · Fig. 3

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Ni-HHTP-250 HRTEM lattice distance	1.85 nm	—	—	Text Exact Reported	399 · Synthesis and characterization · Fig. 3i
Ni-HHTP-250 nanorod diameter	about 50 nm	—	—	Text Approximate	399 · Synthesis and characterization · Fig. 3c,g
Ni-HHTP-250 nanorod length upper bound	1 um	1000 nm	—	Text Range	399 · Synthesis and characterization · Fig. 3c
Ni-HHTP-250 nanorod length lower bound	200 nm	—	—	Text Range	399 · Synthesis and characterization · Fig. 3c

FESEM after cycling

Scanning electron microscopy

Ni-HHTP-250 electrode · Electrode

FESEM images after 100 cycles.

Geometry: post-cycling electrode
Context: composite electrode
Measurement source: 403 · Charge storage mechanism · Fig. 6e,f

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
post-100-cycle morphology retention	hexagonal nanorods retained	—	—	Text Qualitative	403 · Charge storage mechanism · Fig. 6e,f