Diffraction Structure — Turning 2D MOFs into Mixed Ionic-Electronic Conductors via Side Chain Engineering

14 measurement groups · 25 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD [100] reflection FWHM

X-ray diffraction and scattering

Cu-1EG pristine powder · Powder

full-width-at-half-maximum of [100] peak near 3.7 deg

Context: pristine powder
Measurement source: p023 · Supplementary Tables 3-4 · Supplementary Figures 17-18

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
FWHM of [100] reflection	0.5	—	—	SI Table Exact Reported	p023 · Supplementary Tables · Supplementary Table 4

PXRD [100] reflection FWHM

X-ray diffraction and scattering

Cu-2EG pristine powder · Powder

full-width-at-half-maximum of [100] peak near 3.7 deg

Context: pristine powder
Measurement source: p023 · Supplementary Tables 3-4 · Supplementary Figures 17-18

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
FWHM of [100] reflection	0.51	—	—	SI Table Exact Reported	p023 · Supplementary Tables · Supplementary Table 4

PXRD [100] reflection FWHM

X-ray diffraction and scattering

Cu-nBu pristine powder · Powder

full-width-at-half-maximum of [100] peak near 3.7 deg

Context: pristine powder
Measurement source: p023 · Supplementary Tables 3-4 · Supplementary Figures 17-18

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
FWHM of [100] reflection	0.553	—	—	SI Table Exact Reported	p023 · Supplementary Tables · Supplementary Table 4

PXRD [100] reflection FWHM

X-ray diffraction and scattering

Ni-1EG pristine powder · Powder

full-width-at-half-maximum of [100] peak near 3.7 deg

Context: pristine powder
Measurement source: p022 · Supplementary Tables 3-4 · Supplementary Figures 17-18

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
FWHM of [100] reflection	0.42	—	—	SI Table Exact Reported	p022 · Supplementary Tables · Supplementary Table 3

PXRD [100] reflection FWHM

X-ray diffraction and scattering

Ni-2EG pristine powder · Powder

full-width-at-half-maximum of [100] peak near 3.7 deg

Context: pristine powder
Measurement source: p022 · Supplementary Tables 3-4 · Supplementary Figures 17-18

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
FWHM of [100] reflection	0.49	—	—	SI Table Exact Reported	p022 · Supplementary Tables · Supplementary Table 3

PXRD [100] reflection FWHM

X-ray diffraction and scattering

Ni-nBu pristine powder · Powder

full-width-at-half-maximum of [100] peak near 3.7 deg

Context: pristine powder
Measurement source: p022 · Supplementary Tables 3-4 · Supplementary Figures 17-18

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
FWHM of [100] reflection	0.5	—	—	SI Table Exact Reported	p022 · Supplementary Tables · Supplementary Table 3

Pawley refinement of experimental PXRD patterns

X-ray diffraction and scattering

Ni-1EG pristine powder · Powder

measured and calculated PXRD; representative measurement row for series

Context: pristine MOF powders
Measurement source: p003 · Results and Discussion · Figure 2a / Figure S13

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
Cu-1EG Rp	2.06%	—	—	Text Exact Reported	p019 · Supplementary Figure 13 · Supplementary Figure 13
Cu-1EG Rwp	2.63%	—	—	Text Exact Reported	p019 · Supplementary Figure 13 · Supplementary Figure 13
Cu-2EG Rp	1.74%	—	—	Text Exact Reported	p019 · Supplementary Figure 13 · Supplementary Figure 13
Cu-2EG Rwp	2.2%	—	—	Text Exact Reported	p019 · Supplementary Figure 13 · Supplementary Figure 13
Cu-nBu Rp	2.01%	—	—	Text Exact Reported	p019 · Supplementary Figure 13 · Supplementary Figure 13
Cu-nBu Rwp	2.54%	—	—	Text Exact Reported	p019 · Supplementary Figure 13 · Supplementary Figure 13
Ni-1EG Rp	1.70%	—	—	Text Exact Reported	p003 · Results and Discussion · Figure S13
Ni-1EG Rwp	2.18%	—	—	Text Exact Reported	p003 · Results and Discussion · Figure S13
Ni-2EG Rp	2.08%	—	—	Text Exact Reported	p003 · Results and Discussion · Figure S13
Ni-2EG Rwp	2.63%	—	—	Text Exact Reported	p003 · Results and Discussion · Figure S13
Ni-nBu Rp	2.45%	—	—	Text Exact Reported	p003 · Results and Discussion · Figure S13
Ni-nBu Rwp	3.07%	—	—	Text Exact Reported	p003 · Results and Discussion · Figure S13

PXRD [001] reflection analysis

X-ray diffraction and scattering

Cu-1EG pristine powder · Powder

interlayer c-c distance from [001] reflection in 2theta 23-28 deg region

Context: pristine powder
Measurement source: p021 · Supplementary Tables 1-2 · Supplementary Figures 15-16

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
experimental interlayer c-c distance	24.6°; c-c 0.36 nm	—	—	SI Table Exact Reported	p021 · Supplementary Tables · Supplementary Table 2

PXRD [001] reflection analysis

X-ray diffraction and scattering

Cu-2EG pristine powder · Powder

interlayer c-c distance from [001] reflection in 2theta 23-28 deg region

Context: pristine powder
Measurement source: p021 · Supplementary Tables 1-2 · Supplementary Figures 15-16

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
experimental interlayer c-c distance	22.2°; c-c 0.40 nm	—	—	SI Table Exact Reported	p021 · Supplementary Tables · Supplementary Table 2

PXRD [001] reflection analysis

X-ray diffraction and scattering

Cu-nBu pristine powder · Powder

interlayer c-c distance from [001] reflection in 2theta 23-28 deg region

Context: pristine powder
Measurement source: p021 · Supplementary Tables 1-2 · Supplementary Figures 15-16

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
experimental interlayer c-c distance	23.7°; c-c 0.38 nm	—	—	SI Table Exact Reported	p021 · Supplementary Tables · Supplementary Table 2

PXRD [001] reflection analysis

X-ray diffraction and scattering

Ni-1EG pristine powder · Powder

interlayer c-c distance from [001] reflection in 2theta 23-28 deg region

Context: pristine powder
Measurement source: p020 · Supplementary Tables 1-2 · Supplementary Figures 15-16

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
experimental interlayer c-c distance	25.1°; c-c 0.35 nm	—	—	SI Table Exact Reported	p020 · Supplementary Tables · Supplementary Table 1

PXRD [001] reflection analysis

X-ray diffraction and scattering

Ni-2EG pristine powder · Powder

interlayer c-c distance from [001] reflection in 2theta 23-28 deg region

Context: pristine powder
Measurement source: p020 · Supplementary Tables 1-2 · Supplementary Figures 15-16

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
experimental interlayer c-c distance	24.3°; c-c 0.37 nm	—	—	SI Table Exact Reported	p020 · Supplementary Tables · Supplementary Table 1

PXRD [001] reflection analysis

X-ray diffraction and scattering

Ni-nBu pristine powder · Powder

interlayer c-c distance from [001] reflection in 2theta 23-28 deg region

Context: pristine powder
Measurement source: p020 · Supplementary Tables 1-2 · Supplementary Figures 15-16

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
experimental interlayer c-c distance	23.8°; c-c 0.37 nm	—	—	SI Table Exact Reported	p020 · Supplementary Tables · Supplementary Table 1

variable-temperature PXRD

X-ray diffraction and scattering

Ni-1EG pristine powder · Powder

ambient air thermal stability assessment

Temperature: 298-573
Atmosphere: ambient air
Context: pristine Ni-1EG
Measurement source: p004 · Results and Discussion · Figure S22

Property	Reported value	Normalised value	Uncertainty	Origin and quality	Source
temperature retaining characteristic PXRD peaksMarked as a best value within this paper	up to 250 °C	—	—	Text Rounded Reported	p004 · Results and Discussion · Figure S22