Other — Bimetallic MOFs with tunable morphology: Synthesis and enhanced lithium storage properties

Measurement evidence

Other

Bimetallic MOFs with tunable morphology: Synthesis and enhanced lithium storage properties · He S., Li Z., Wang J. · Journal of Solid State Chemistry · 2022 · 122726

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Inductively coupled plasma optical emission spectrometry (ICP-OES, Agilent 720 ES)

Co-Ni-MOF/Ni-MOF powder series · Powder

Determination of precise Co/Ni ratios in the as-synthesised powders.

Context
pristine powder series
Measurement source
2 · 2.1. Preparation of Co-Ni-MOF
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Actual Co/Ni ratio for nominal 1:1 sampleMarked as a best value within this paperCo/Ni about 1:0.90Text
Rounded Reported
2 · 2.1. Preparation of Co-Ni-MOF
Actual Co/Ni ratio for nominal 1:2 sampleCo/Ni about 1:1.64Text
Rounded Reported
2 · 2.1. Preparation of Co-Ni-MOF
Actual Co/Ni ratio for nominal 2:1 sampleCo/Ni about 1:0.48Text
Rounded Reported
2 · 2.1. Preparation of Co-Ni-MOF

Thermogravimetric analysis, STA 449C thermal analyser

Co-Ni-MOF/Ni-MOF powder series · Powder

TGA of MOF powders in nitrogen.

Atmosphere
nitrogen
Context
pristine powder series
Measurement source
2 · 2.2. Characterization · Fig. 1d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TGA main framework breakdown temperaturemassive weight loss at around 420 deg C assigned to complete breakdown of BDC ligandsaroundText
Approximate
3 · 3. Results and discussion · Fig. 1d
Thermal stability comparisonCo-Ni-MOF materials show considerably improved thermal stability compared with single Ni-MOF.Text
Qualitative
3 · 3. Results and discussion · Fig. 1d