Other — Novel semiconducting metal-organic framework: Synthesis, structural characterisation and electrical conductivity studies of manganese based two dimensional coordination polymer

Measurement evidence

Other

Novel semiconducting metal-organic framework: Synthesis, structural characterisation and electrical conductivity studies of manganese based two dimensional coordination polymer · Karthikeyan M., Bhagyaraju B., Mariappan C.R. et al. · Inorganic Chemistry Communications · 2012 · 269-272

1 measurement group · 7 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

Thermogravimetric analysis

Pale yellow [Mn(mu-pz)(mu-Cl)2]n crystals · Single Crystal

Heated from 40 to 700 C in air at 10 C min-1.

Atmosphere
air
Context
pristine framework
Measurement source
269 · Thermogravimetric analysis · Fig. S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
TGA end temperature700 C973.15 KText
Exact Reported
269 · Thermogravimetric analysis
TGA heating rate10 C min-1Text
Exact Reported
269 · Thermogravimetric analysis
Approximate TGA curve value after first major stepapproximately 52% at about 420 C from Fig. S1visual estimate from rendered axisVisual Estimate
Approximate
2 · Supporting Information · Fig. S1
Approximate TGA curve value before major mass-loss stepapproximately 97% at about 310 C from Fig. S1visual estimate from rendered axisVisual Estimate
Approximate
2 · Supporting Information · Fig. S1
Approximate final TGA curve valueapproximately 31% near 690 C from Fig. S1visual estimate from rendered axisVisual Estimate
Approximate
2 · Supporting Information · Fig. S1
Thermal stability limitMarked as a best value within this paperstable up to 310 C583.15 KText
Rounded Reported
269 · Thermogravimetric analysis · Fig. S1
TGA start temperature40 C313.15 KText
Exact Reported
269 · Thermogravimetric analysis