Complete recipeSource: Main
Route 1: Other
272 · Reference note [12]
Metal precursorsmanganese chloride tetra hydrate, 395.8 mg, 2 mmol
Linker precursorspyrazine, 160 mg, 2 mmol
Solventsdistilled water, 2 ml; ethanol-water mixture, 2 ml
AtmosphereAmbient atmosphere; not otherwise controlled
Temperatureambient temperature
Time168
Work-upCrystals were washed with distilled water and ethanol, filtered and dried in vacuum.
ActivationVacuum drying after filtration; no separate activation reported.
Scalability contextSmall-batch ambient crystallisation; isolated yield 520 mg (95%).
Show 4 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | manganese chloride tetra hydrate | 395.8 mg, 2 mmol · in distilled water (2 ml) | 272 · Reference note [12] |
| Linker | pyrazine | 160 mg, 2 mmol · in ethanol-water mixture (2 ml) | 272 · Reference note [12] |
| Solvent | distilled water | 2 ml | 272 · Reference note [12] |
| Solvent | ethanol-water mixture | 2 ml · ethanol:water ratio not reported | 272 · Reference note [12] |