Microscopy Morphology — Novel CoS2 embedded carbon nanocages by direct sulfurizing metal-organic frameworks for dye-sensitized solar cells

Measurement evidence

Microscopy Morphology

Novel CoS2 embedded carbon nanocages by direct sulfurizing metal-organic frameworks for dye-sensitized solar cells · Cui X., Xie Z., Wang Y. · Nanoscale · 2016 · 11984-11992

3 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

SEM

CoS2_4 h CE · Electrode

SEM comparison of sulfurisation-time series before and after annealing

Context
MOF-derived CoS2/carbon samples
Measurement source
11986 · Results and discussion · Fig. 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
CoS2_4 h hollow sphere diameterMarked as a best value within this paper~500 nm5e-7 mText
Approximate
11986 · Results and discussion · Fig. 1g
CoS2_4 h wall thicknessMarked as a best value within this paper~20 nm2e-8 mText
Approximate
11986 · Results and discussion · Fig. 1g

SEM

as-prepared ZIF-67 · Powder

FEI Quanta 3D FEG SEM; morphology of as-prepared ZIF-67 template

Context
pristine ZIF-67 template control
Measurement source
11985 · 2.4 Characterization and measurement · Fig. 1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
ZIF-67 average particle sizeabout 500 nm5e-7 mText
Approximate
11986 · Results and discussion · Fig. 1a

TEM/HRTEM/SAED

CoS2_4 h CE · Electrode

JEM-1400 TEM at 120 kV; HRTEM and SAED for CoS2 embedded carbon nanocages

Context
MOF-derived CoS2/carbon nanocages
Measurement source
11988 · Results and discussion · Fig. 5
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
CoS2 nanocrystal diameterMarked as a best value within this paper~5 nm5e-9 mText
Approximate
11988 · Results and discussion · Fig. 5b
HRTEM lattice spacing assigned to CoS2 (311)1.670 A0.167 nmText
Exact Reported
11988 · Results and discussion · Fig. 5b