SEM, TEM, XRD
D-Fe2O3-NSA microrods · Powder
D-Fe2O3-NSA comparison after oxidation at 350 deg C
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|
Microscopy Morphology — Electrochemical properties of uniquely structured Fe2O3 and FeSe2/graphitic-carbon microrods synthesized by applying a metal-organic framework
Measurement evidence
Microscopy Morphology
Electrochemical properties of uniquely structured Fe2O3 and FeSe2/graphitic-carbon microrods synthesized by applying a metal-organic framework · Park S.-K., Kim J.K., Kang Y.C. · Chemical Engineering Journal · 2018 · 2440-2449
3 measurement groups · 4 results
Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.
SEM, TEM, XRD, Raman spectroscopy
Raman spectroscopyX-ray diffraction and scatteringScanning electron microscopyTransmission electron microscopy
D-FeSe2/C microrods · Powder
Dense FeSe2/C comparison sample prepared by direct selenization of MIL-88
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| mean primary FeSe2 particle size | 8.2 nm | — | — | Text Exact Reported | p006 / journal p2445 · Results & discussion · Figs. S10 and S8 referenced |
| Raman ID/IG ratio | 1.05 | — | — | Text Exact Reported | p006 / journal p2445 · Results & discussion · Fig. S11 referenced |
SEM, TEM, HR-TEM, SAED, elemental mapping, XRD
X-ray diffraction and scatteringScanning electron microscopyTransmission electron microscopyElemental microanalysis and mapping
Fe@GC microrods · Powder
Fe@GC microrods after reduction at 450 deg C under H2/Ar
| Property | Reported value | Normalised value | Uncertainty | Origin and quality | Source |
|---|---|---|---|---|---|
| HR-TEM d-spacing assigned to metallic Fe (110) | 0.20 nm | — | — | Text Exact Reported | p003 / journal p2442 · Results & discussion · Fig. 1e |
| HR-TEM d-spacing assigned to Fe2O3 (104) | 0.27 nm | — | — | Text Exact Reported | p003 / journal p2442 · Results & discussion · Fig. 1e |