Partial recipeSource: Both
Route 1: Other
SI text · Experimental Section/Methods - Synthesis of Cu-BHT
Metal precursorsCuCl2 dissolved in DI water to yield different concentration Cu ion solutions; 70 wt.% CuCl2 selected for further investigation
Linker precursorsBHT dissolved in chlorobenzene to form a 0.5 mM BHT solution
SolventsDI water; chlorobenzene; ethanol wash; DI water wash
Additives10 wt% NaOH for cotton desizing and cleaning
Atmosphereair / fume hood drying; no inert atmosphere reported
TimeNaOH pretreatment overnight; Cu ion soak 4 h; BHT reaction 0.5 h
Substrate orientationcotton textile immersed/soaked; BHT solution applied to cover Cu-cotton samples
Work-upAir-dried in a fume hood after Cu soak; after BHT reaction washed with EtOH and DI water.
Scalability contextSimple modification of common fabrics by soaking/coating; volumes, fabric size, and exact CuCl2 solution concentrations for each sample are not fully specified.
Show 6 structured reagent records
| Role | Reagent | Amount / concentration | Source |
|---|---|---|---|
| Metal Source | Copper chloride (CuCl2) | different concentration Cu ions solution; 70 wt.% selected in main text | SI text · Experimental Section/Methods - Synthesis of Cu-BHT |
| Linker | 1,2,3,4,5,6-benzenehexathiol (BHT) | 0.5 mM in chlorobenzene | SI text · Experimental Section/Methods - Synthesis of Cu-BHT |
| Solvent | chlorobenzene (CB) | Not specified | SI text · Experimental Section/Methods - Synthesis of Cu-BHT |
| Solvent | deionized water (DI water) | Not specified | SI text · Experimental Section/Methods - Synthesis of Cu-BHT |
| Base | NaOH | 10 wt% | SI text · Experimental Section/Methods - Synthesis of Cu-BHT |
| Solvent | Ethanol (EtOH) | wash solvent | SI text · Experimental Section/Methods - Synthesis of Cu-BHT |