cMOF Evidence Base
Diffraction Structure — Highly Conductive Two-Dimensional Metal-Organic Frameworks for Resilient Lithium Storage with Superb Rate Capability

Measurement evidence

Diffraction Structure

Highly Conductive Two-Dimensional Metal-Organic Frameworks for Resilient Lithium Storage with Superb Rate Capability · Wu Z., Adekoya D., Huang X. et al. · ACS Nano · 2020 · 12016-12026

2 measurement groups · 5 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

PXRD after solvent/chemical soaking

X-ray diffraction and scattering

as-prepared Cu-BHT powder · Powder

10 mg sample ultrasonically dispersed into 3 mL solvent for 10 min, stood for 25 h, washed with H2O and acetone

Context
pristine framework powder
Measurement source
p004 / 12019 · Materials Characterization and Stability Evaluation · Figure 1b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
chemical/electrolyte stabilitywell-maintained crystallinity after base, acid, hot water, carbonate electrolyte and ether electrolyte exposure for 25 h——Text
Qualitative		p004 / 12019 · Materials Characterization and Stability Evaluation · Figure 1b

PXRD with structure simulation/Rietveld refinement

X-ray diffraction and scattering

as-prepared Cu-BHT powder · Powder

as-prepared 2D Cu-BHT powder; simulated and experimental patterns compared

Context
pristine framework powder
Measurement source
p004 / 12019 · Materials Characterization and Stability Evaluation · Figure S1
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Rietveld-refined lattice a=bMarked as a best value within this papera = b = 8.45 A——Text
Exact Reported		p004 / 12019 · Materials Characterization and Stability Evaluation · Figure S1
simulated lattice a=ba = b = 8.8 A——Text
Rounded Reported		p004 / 12019 · Materials Characterization and Stability Evaluation · Figure S1
simulated lattice cc = 20 A——Text
Rounded Reported		p004 / 12019 · Materials Characterization and Stability Evaluation · Figure S1
space groupP6/mmm——Text
Exact Reported		p004 / 12019 · Materials Characterization and Stability Evaluation · Figure S1