Microscopy Morphology — Enhancing electrochemical hydrogen storage in nickel-based metal-organic frameworks (MOFs) through zinc and cobalt doping as bimetallic MOFs

Measurement evidence

Microscopy Morphology

Enhancing electrochemical hydrogen storage in nickel-based metal-organic frameworks (MOFs) through zinc and cobalt doping as bimetallic MOFs · Kashani F.Z., Mohsennia M. · International Journal of Hydrogen Energy · 2025 · 348-357

4 measurement groups · 10 results

Reported values remain attached to the sample, method, conditions, extraction quality and source location that produced them.

EDS/EDX elemental analysis and mapping coupled with FESEM

Co-Ni(TPA)-2 · Powder

EDX spectrum and elemental mapping for Co-Ni(TPA)-2.

Geometry
powder
Context
Co-doped Ni(TPA)
Measurement source
350 · 3.1. Characterization of synthesized MOFs · Figs. 3 and 4
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Co atomic content by EDXCo At (%) = 5.89Visual Estimate
Rounded Reported
352 · Figure page · Fig. 3 inset table
Co/Ni ratioCo/Ni ratio = 0.78Text
Rounded Reported
350 · 3.1. Characterization of synthesized MOFs · Fig. 3
Co content by EDXCo Wt (%) = 17.25Visual Estimate
Rounded Reported
352 · Figure page · Fig. 3 inset table
Ni atomic content by EDXNi At (%) = 7.54Visual Estimate
Rounded Reported
352 · Figure page · Fig. 3 inset table
Ni content by EDXNi Wt (%) = 22.19Visual Estimate
Rounded Reported
352 · Figure page · Fig. 3 inset table

FE-SEM

Co-Ni(TPA)-2 · Powder

Low and high magnification SEM images.

Geometry
powder
Context
Co-doped Ni(TPA)
Measurement source
351 · 3.1. Characterization of synthesized MOFs · Fig. 2e,f
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Morphologyregular petal-like sheetsText
Qualitative
350 · 3.1. Characterization of synthesized MOFs · Fig. 2e,f

FE-SEM

Ni(TPA) · Powder

Low and high magnification SEM images.

Geometry
powder
Context
pristine Ni(TPA)
Measurement source
351 · 3.1. Characterization of synthesized MOFs · Fig. 2a,b
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Morphologysignificant number of nanosheetsText
Qualitative
350 · 3.1. Characterization of synthesized MOFs · Fig. 2a

FE-SEM

Zn-Ni(TPA)-2 · Powder

Low and high magnification SEM images.

Geometry
powder
Context
Zn-doped Ni(TPA)
Measurement source
351 · 3.1. Characterization of synthesized MOFs · Fig. 2c,d
PropertyReported valueNormalised valueUncertaintyOrigin and qualitySource
Average distance between adjacent nanosheets in bimetallic samplesabout 45 nmText
Approximate
350 · 3.1. Characterization of synthesized MOFs · Fig. 2
Average sheet thickness in bimetallic samplesabout 22 nmText
Approximate
350 · 3.1. Characterization of synthesized MOFs · Fig. 2
Morphologyregular petal-like sheetsText
Qualitative
350 · 3.1. Characterization of synthesized MOFs · Fig. 2c,d